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		<id>https://e-learning.pan-training.eu/wiki/index.php?title=Spectrometers:_Instruments_for_inelastic_neutron_scattering&amp;diff=1160&amp;oldid=prev</id>
		<title>ucph&gt;Tommy at 14:33, 29 August 2019</title>
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		<updated>2019-08-29T14:33:04Z</updated>

		<summary type="html">&lt;p&gt;&lt;/p&gt;
&lt;p&gt;&lt;b&gt;New page&lt;/b&gt;&lt;/p&gt;&lt;div&gt;On instruments that use a continuous beam of neutrons, it is necessary to&lt;br /&gt;
directly select both \(E_{\rm i}\) and \(E_{\rm f}\), in order to determine&lt;br /&gt;
the neutron energy transfer, \(\hbar\omega\). It is here&lt;br /&gt;
customary to use Bragg diffraction from crystals for both purposes.&lt;br /&gt;
Such a type of instrument is denoted a triple-axis spectrometer,&lt;br /&gt;
since the neutron changes direction by scattering three times before&lt;br /&gt;
being detected:&lt;br /&gt;
&lt;br /&gt;
* A monochromator crystal selects \(E_{\rm i}\) of the incoming beam, as discussed in [[Determining the incoming neutron wavelength]], by Bragg scattering an angle \(2\theta_{\rm m}\).&lt;br /&gt;
* The sample scatters the beam by the angle \(2\theta\).&lt;br /&gt;
* The analyzer determines \(E_{\rm f}\) by Bragg scattering by an angle \(2\theta_{\rm a}\), in the same way as the monochromator.&lt;br /&gt;
&lt;br /&gt;
The path of the neutron beam is kept in the same horizontal plane,&lt;br /&gt;
also denoted the scattering plane.&lt;br /&gt;
The build-up of the triple-axis spectrometer is shown in &amp;lt;xr id=&amp;quot;fig:tripleaxisspectrometer&amp;quot;&amp;gt;Figure %i&amp;lt;/xr&amp;gt;, and the individual &lt;br /&gt;
components of the spectrometer are listed below:&lt;br /&gt;
&lt;br /&gt;
&amp;lt;figure id=&amp;quot;fig:tripleaxisspectrometer&amp;quot;&amp;gt;[[File:tripleaxisspectrometer.png|thumb|600px|&amp;lt;caption&amp;gt;A sketch of a triple-axis spectrometer, showing the three scattering angles, \(2\Theta_m\), \(2\Theta\) and \(2\Theta_a\). The monochromator and analyser both select a single wavelength by Bragg diffraction from a single crystal. The instrument also contains a number of slits, collimators, and filters to shape the beam.&amp;lt;/caption&amp;gt;]]&amp;lt;/figure&amp;gt;&lt;br /&gt;
&lt;br /&gt;
====Source====&lt;br /&gt;
The triple axis spectrometer uses a beam of cold or thermal neutrons. Most usually, a neutron guide &lt;br /&gt;
is used to transport the beam to areas far from the source where the stray background is lower.&lt;br /&gt;
====Monochromator====&lt;br /&gt;
The beam is diffracted by a monochromator (see subsection [[Determining the incoming neutron wavelength]]), &lt;br /&gt;
which selects the neutron energy, \(E_{\rm i}\), typically in the range 14-100~meV at a thermal moderator,&lt;br /&gt;
or 2.5-14~meV for a cold moderator.&lt;br /&gt;
====Filter==== &lt;br /&gt;
The monochromatised beam is almost always polluted with higher order scattering, from \(n&amp;gt;1\) in Bragg&amp;#039;s law.&lt;br /&gt;
A filter is used to remove these higher order scattered neutrons, either before or after the sample, or in both places.&lt;br /&gt;
====Collimator====&lt;br /&gt;
The monochromatic beam passes through a (often loosely collimating) horizontal Soller collimator. Collimators&lt;br /&gt;
may also be inserted before the monochromator (rarely), between sample and analyzer (often), and after the analyzer (sometimes).&lt;br /&gt;
====Sample====&lt;br /&gt;
The medium-divergent, monochromatic beam hits the sample, which is often one (or several co-aligned) single crystal situated in a vacuum&lt;br /&gt;
environment to reduce background from air scattering. In the sample, the neutrons are scattered elastically and inelastically.&lt;br /&gt;
====Analyser====&lt;br /&gt;
The scattered beam is again monochromatized by the analyser crystal, which works just like a monochromator, just selecting &lt;br /&gt;
the final neutron energy, \(E_{\rm f}\). Usually, pyrolytic graphite is used for analyzer material.&lt;br /&gt;
====Detector====&lt;br /&gt;
The scattered neutrons are eventually detected by a single detector. This means that data on a triple-axis spectrometer are taken point by point. More advanced spectrometers may have several analyzer-detector arrangements, allowing for simultaneously detecting several points in&lt;br /&gt;
\(({\bf q},\omega)\)-space. &amp;lt;ref name=&amp;quot;rodriguez08&amp;quot;&amp;gt;J.A. Rodriguez et al. Macs - a new high intensity cold neutron spectrometer at nist. Meas. Sci Techn., 19:034023, 2006.&amp;lt;/ref&amp;gt;&amp;lt;ref name=&amp;quot;lefmann06&amp;quot;&amp;gt;K. Lefmann et al. Realizing the full potential of a rita spectrometer. Physica B, 385-386:1083-1085, 2006.&amp;lt;/ref&amp;gt;&amp;lt;ref name=&amp;quot;kempa06&amp;quot;&amp;gt;M. Kempa et al. The flatcone multianalyzer setup for ill&amp;#039;s three-axis spectrometers. Physica B, 385-386:1080, 2006.&amp;lt;/ref&amp;gt;&lt;br /&gt;
&lt;br /&gt;
&lt;br /&gt;
By correct selection of the three scattering angles, and the sample rotation, \(\omega_{\rm s}\), around a vertical axis, &lt;br /&gt;
the triple-axis spectrometer can be adjusted to any value of&lt;br /&gt;
scattering vector, \({\bf q}\), and energy transfer, \(\hbar \omega\),&lt;br /&gt;
allowed by the scattering condition (\ref{eq:inelastic_basic}).&lt;br /&gt;
In fact, \({\bf q}\) can only obtain values within the scattering plane.&lt;br /&gt;
This means that there are 4 free angles to determine only 3 parameters:&lt;br /&gt;
\(\hbar \omega\) and 2 dimensions of \({\bf q}\). In practice, this ambigiuity&lt;br /&gt;
is solved by fixing either \(E_{\rm i}\) or \(E_{\rm f}\) to a predetermined value.&lt;br /&gt;
&lt;br /&gt;
A thorough presentation of how to perform experiments with a triple-axis&lt;br /&gt;
spectrometer is given in Ref.~\cite{shirane}.&lt;br /&gt;
&lt;br /&gt;
====Experimental considerations==== &lt;br /&gt;
The 3 scattering angles, &lt;br /&gt;
\(2\theta_{\rm m}\), \(2\theta\), and \(2\theta_{\rm a}\), are often denoted&lt;br /&gt;
by the less-obvious symbols \(A2\), \(A4\), and \(A6\), respectively.&lt;br /&gt;
The symbol \(A3\) denotes the sample rotation \(\omega_{\rm s}\), while the&lt;br /&gt;
symbols \(A1\) and \(A5\) denotes the rotation of monochromator and analyzer&lt;br /&gt;
crystals, respectively. This is also listed in table \ref{tab:As}.&lt;br /&gt;
&lt;br /&gt;
&amp;lt;figtable id=&amp;quot;tab:rotationangletable&amp;quot;&amp;gt;[[File:rotationangletable.PNG| thumb | 300px |&amp;lt;caption&amp;gt;Different notations for rotations angles in a triple-axis spectrometer.]]&amp;lt;/figtable&amp;gt;&lt;br /&gt;
&lt;br /&gt;
Often, an experimental series consists of scans along a particular axis&lt;br /&gt;
in \(({\bf q},\hbar\omega)\) space. One speaks about constant-energy scans&lt;br /&gt;
and constant-q scans. For the latter, it is costumary to use a constant&lt;br /&gt;
\(E_{\rm f}\) for the scans and then measure each scan point &lt;br /&gt;
until a constant count number in the beam monitor has been reached.&lt;br /&gt;
Since the sensitivity of the monitor is proportional to wavelength, &lt;br /&gt;
\(\lambda_{\rm i}\), the number of neutrons reaching the sample for each &lt;br /&gt;
scan point is proportional to \(1/\lambda_{\rm i}\) - or to \(k_{\rm i}\).&lt;br /&gt;
These facts causes the factor \(k_{\rm f}/k_{\rm i}\) &lt;br /&gt;
in the final cross section (\ref{eq:master_scatt_inel}) to be constant.&lt;br /&gt;
Hence, the variation of this factor can be neglected, &lt;br /&gt;
easing the subsequent data analysis.&lt;br /&gt;
&lt;br /&gt;
==Two types of spectrometers for a pulsed source==&lt;br /&gt;
On instruments at pulsed sources, &lt;br /&gt;
one can utilize time-of-flight techniques as for diffraction.&lt;br /&gt;
However, the time-of-flight cannot be used to determine both &lt;br /&gt;
\(E_{\rm i}\) and \(E_{\rm f}\). Either the initial or final energy &lt;br /&gt;
must be selected by other means, typically&lt;br /&gt;
by Bragg reflection from crystals or by chopping the beam in short time pulses&lt;br /&gt;
close to the sample.&lt;br /&gt;
This leads to two essentially different types of spectrometer geometries:&lt;br /&gt;
&lt;br /&gt;
====Direct geometry==== &lt;br /&gt;
The incoming neutrons are monochromatized by a chopper system and hits the sample in a short burst. Thus, \(E_{\rm i}\) is fixed, and the time-of-flight is used to determine the value of \(E_{\rm f}\).&lt;br /&gt;
====Indirect geometry====&lt;br /&gt;
The sample is hit by a &amp;quot;white&amp;quot; beam, and only outgoing neutrons with a particular energy are scattered by analyzer crystals on to the detector. Thus, \(E_{\rm f}\) is fixed and the time-of-flight is used to determine the value of \(E_{\rm i}\).&lt;br /&gt;
&lt;br /&gt;
The advantages with time-of-flight spectroscopy are so large, that at&lt;br /&gt;
many continuous sources one chooses to chop the beam close to the source,&lt;br /&gt;
producing short pulses. In this way more than 99% of the neutrons coming through the guide system are sacrificed.&lt;br /&gt;
&lt;br /&gt;
In later versions of these notes, there will be more material on&lt;br /&gt;
time-of-flight spectrometers, including figures.&lt;/div&gt;</summary>
		<author><name>ucph&gt;Tommy</name></author>
	</entry>
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